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ISSN : 1598-6616(Print)
ISSN : 2287-6731(Online)
Journal of Korean Society of Odor Research and Engineering Vol.5 No.4 pp.226-236
 

해드스페이스-GC/FID를 이용한 대기 중 트라이메틸아민 분석법 개발

Abstract

An analytical method for trimethylamine in ambient air was developed, using headspace gas chromatography with flame ionization detection. Trimethylamine was collected on the acid filter which was impregnated sulfuric aicd in the 47 ㎜ diameter of glass fiber filter. Trimethylamine collected on the acid filter was regenerated in the headspace vial and introduced into the GC analytical column directly. Several parameters such as sample volume, equilibrium temperature and time, and slurry method of filter were optimized to provide maximum detection response. Resolution power also compared according to liquid phase of analytical column. The detection limit of method was 0.13 ppb with 50 L sampling volume. The developed acid filter method is easy to deal with the field sampling and the method was adopted as the standard method for odor analysis in Korea.

해드스페이스-GC/FID를 이용한 대기 중 트라이메틸아민 분석법 개발

김만구,박수미,정탁교,장미옥,이철원,이민도,한진석

초록